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APEXII Training
Practical guide to screen crystals,collect data, solve and refinestructures for the APEXII®program suite
Joseph H. Reibenspies
Department of Chemistry
Texas A & M University
This presentation is narrated
All rights reserved.  Please do not copy, modify or distribute theseslides without the consent of the authors.
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Notes
On-line Lectures
FLASH movie or HTML5 (ISPRING)
STOP presentation at any time
Time :  ~ 1 hour
Practicals for BRUKER AXS users
Mistakes and errors
Contact Joseph Reibenspies
xray@tamu.edu
Texas A & M assumes no liability or responsibility for any errors oromissions in the content of this set of lectures.
These lectures are intended for use for registered students of Texas A & MUniversity.
Other students are welcome
Access to and use of the materials in this course is free for personal, non-commercial use only.  Distribution of this material is prohibited.
To Exit and Return
Use your Brower’s  BACK key to return to the Lecture Menu Website.
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Getting Started
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BIS is not running???
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Start your project
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Note on Project names ::   Group nomenclature :
Example :   P.I.’s initials_date_projectname
JHR_2015_10_4_CuI2
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Setup
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Tabs:  Followthem in order
Tabs:  Followthem in order
Describe
Describe
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Describe Compound
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Compound Name
Compound Name
Formula
Formula
Crystal Color
Crystal Color
Crystal Shape
Crystal Shape
Leave crystal dimensionboxes  blank for now
Leave crystal dimensionboxes  blank for now
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Center
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C:\Users\jhr6675\Pictures\2015-03-02 center\center 003.JPG
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Evaluate
Automatic Mode
Automatic Mode
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Collect “Matrix”
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Frames
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Harvesting “spots”
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Indexing
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Indexing
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Index results
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Higher the score the
better the solution.
ALSO
If both cells are the
same then you most
likely have the solution.
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Refining the unit cell
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Bravais Lattice
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FOM = 1
Good
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Unit Cell
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Right clickin framefor spottools
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Collect Data
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Data Collection
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Data Collection
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Right click
Right click
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Integration
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The integration
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Crystal Faces
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Scale
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Examine Data
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Solve Structure
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Solution
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Refinement
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Report
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End of Training
Questions?
Thank you for listening
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